By Bhushan, Vikas

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Soc. p . 727 (1942). N . A. Milas, S. W. Lee, E. Sakal, H. C. Wohlers, N . S. MacDonald, F . X . Grossi, and H. F . Wright, / . Am. Chem. Soc. 70, 1584 (1948). Farbenfabriken Bayer A. , German P a t e n t 1,142,595 (1963); see also H. Oediger and K. Eiter, Chem. Ber. 97, 549 (1964). Farbenfabriken Bayer A. , German P a t e n t 1,157,606 (1964). J. Cymerman, I. M. Heilbron, and E . R. H. Jones, J. Chem. Soc. p . 90 (1945). II. CHEMISTRY 35 36 1. ,143 allows the synthesis of three isomers: all-trans- (XVI), 11-eis- (XLIX), and 11,13di-as-vitamin A (XLVIII).

H. Jones, and A. Spinks, J. Chem. Soc. p . 727 (1942). N . A. Milas, S. W. Lee, E. Sakal, H. C. Wohlers, N . S. MacDonald, F . X . Grossi, and H. F . Wright, / . Am. Chem. Soc. 70, 1584 (1948). Farbenfabriken Bayer A. , German P a t e n t 1,142,595 (1963); see also H. Oediger and K. Eiter, Chem. Ber. 97, 549 (1964). Farbenfabriken Bayer A. , German P a t e n t 1,157,606 (1964). J. Cymerman, I. M. Heilbron, and E . R. H. Jones, J. Chem. Soc. p . 90 (1945). II. CHEMISTRY 35 36 1. ,143 allows the synthesis of three isomers: all-trans- (XVI), 11-eis- (XLIX), and 11,13di-as-vitamin A (XLVIII).

64-82> 113 Neither the retinol nor the retinal series show charac­ teristic differences for the various isomers. The spectrum of all-/remsvitamin A is shown in Fig. 02 mm). c. 43 A temperature effect has been ob­ served in the case of 11,13-di-cis-vitamin A. 43 The spectrum of all-^rans-vitamin A is shown in Fig. 4. 112 113 See ref. 321. W. Oroshnik, / . Am. Chem. Soc. 78, 2651 (1956). 24 1. VITAMINS A AND CAROTENE F I G . 4. Nuclear magnetic resonance spectrum (60 Mc/sec) of all-£rans-vitamin A (in CDC1 3 ).

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